Process Validation

Agenda: Day One

 

I. Examine the Fundamentals of Process Validation

• Define key terminology and common acronyms

• Explain what, when, how and why we validate and qualify processes

• Determine the key components of process validation and the validation Lifecycle

II. Comply with Regulatory Requirements for Process Validation

• Review GxPs as related to production and process controls

• Clarify the different levels of validation required by FDA

• Determine the implications of not performing validation and qualification

• Assess latest regulatory trends and identify validation red flagsExercise: Critique Sample 483s and Warning Letters

III. Conduct Process Validation and Equipment Qualification

•Write IQ/OQ/PQ protocols for production processes and equipment

• Perform equipment qualification activities

• Use validation guides, templates and worksheets to collect data

• Learn different methodologies for qualifying equipment and determiningcritical process parameters

IV. Develop and Maintain Adequate Documentation Systems

• Analyze documentation requirements for validation projects

• Examine the Big Three: Validation Master Plan, Validation SOP andValidation Protocol/Summary ReportExercise: Examine and Evaluate a Sample Validation Master Plan

V. Determine the Format and Function of a Validation Protocol

• Outline the parameters and criteria for validation protocols

• Determine the objectives of validation and qualification studies

• Develop and execute various protocols

• Set appropriate acceptance criteria and specifications

• Assess the importance of statistics and quality tools and their relationshipto process validationExercise: Review Sample Validation Protocols

Agenda: Day Two

VI. Develop an Accurate Validation Summary Report

• Determine what to include in the validation report

• Build an appropriate timeline for validation report completion

• Ensure results meet acceptance criteria and testing objectives

• Learn what FDA investigators are looking for when assessing yourvalidation documentationExercise:

Assess Validation Needs by Conducting a GAP Analysis

VII. Establish Effective Validation Programs

• Explain in detail the FDA’s current systems-based inspection strategy

Implement current industry best practices for developing and deployingvalidation programs

• Explain how to perform process validation with emphasis on the validationlifecycleExercise: Analyze Case Studies to Define Requirements for Validation

VIII. Apply Risk Analysis to Process Validation

• Determine the benefits of applying risk analysis in your validation plan

• Review the FDA’s risk-based approach as it relates to validation activities

• Define current industry standard

• Apply risk management principles when selecting validation targetsIX. Monitor and Control Your Validated Processes

• Differentiate between prospective, concurrent and retrospectivevalidation and qualification

• Clarify the difference between revalidation and post-validation monitoringactivities

• Determine what changes should be validated and/or verified

• Comply with FDA expectations for annual product reviews, design

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